目錄
Preface
前言
Chapter 1 Introduction 緒論 1
1.1 Chemistry Laboratory Safety Policies 化學(xué)實(shí)驗(yàn)室安全制度 1
1.2 Requirements for the Course 課程要求 6
1.3 Guidelines for Lab Notebook, Pre-lab, and Post-lab Report 實(shí)驗(yàn)記錄本、預(yù)習(xí)報(bào)告和實(shí)驗(yàn)報(bào)告指南 9
1.4 Introduction to Titrimetric Analysis 滴定分析法概述 12
1.5 Significant Figures and Data Treatment 有效數(shù)字和數(shù)據(jù)處理 16
Chapter 2 Basic Operations and Common Instruments 基本操作和常用儀器 22
2.1 Cleaning and Drying Glassware 玻璃器皿的洗滌和干燥 22
2.2 Transferring Reagents 試劑的取用 24
2.3 Use of Volumetric Glassware 量器類(lèi)玻璃器皿的使用 25
2.4 Separation Techniques 分離技術(shù) 32
2.5 Common Instruments 常用儀器 36
Chapter 3 Fundamental Inorganic Chemistry Experiments 基礎(chǔ)無(wú)機(jī)化學(xué)實(shí)驗(yàn) 47
Expt. 1 Separation and Identification of Common Cations 常見(jiàn)陽(yáng)離子的分離和鑒定 47
Expt. 2 Separation and Identification of Common Anions 常見(jiàn)陰離子的分離和鑒定 53
Expt. 3 Determination of Reaction Rate Constant, Activation Energy and Influencing Factors 反應(yīng)速率常數(shù)、活化能及影響因素的測(cè)定 60
Expt. 4 Preparation of Alum and Large Crystal Cultivation 明礬的制備及其大晶體培養(yǎng) 66
Chapter 4 Fundamental Analytical Chemistry Experiments 基礎(chǔ)分析化學(xué)實(shí)驗(yàn) 72
Expt. 5 Preparation and Standardization of the Solutions for Acid-base Titration 酸堿滴定溶液的配制與標(biāo)定 72
Expt. 6 Preparation and Standardization of the Solutions for Redox Titration 氧化還原滴定溶液的配制與標(biāo)定 77
Expt. 7 Preparation and Standardization of the Solution for Complexometric Titration 配位滴定溶液的配制與標(biāo)定 84
Expt. 8 Preparation and Standardization of the Solution for Precipitation Titration 沉淀滴定溶液的配制與標(biāo)定 88
Expt. 9 Practise of Basic Operations for Titrimetric Analysis 滴定分析基本操作訓(xùn)練 92
Expt. 10 Determination of the Molecular Weight of an Unknown Diprotic Organic Acid 未知二元有機(jī)酸分子量的測(cè)定 95
Chapter 5 Comprehensive and Designing Experiments 綜合設(shè)計(jì)實(shí)驗(yàn) 98
Expt. 11 Determination of the Fluoride Content in Tea Samples by FISE 氟離子選擇電極法測(cè)定茶葉中氟離子含量 98
Expt. 12 Preparation and Characterization of Mohr’s Salt 莫爾鹽的制備及表征 104
Expt. 13 Preparation and Characterization of Copper Methionine 蛋氨酸銅的制備及表征 107
Expt. 14 Preparation and Photosensitivity Test of Potassium Trioxalatoferrate(III) Trihydrate 三水合三草酸合鐵(III)酸鉀的制備及光敏性測(cè)試 111
Expt. 15 Determination of the Charge Number of Trioxalatoferrate(III) Complex Ion 三草酸合鐵(III)配離子電荷數(shù)的測(cè)定 115
Expt. 16 Spectrophotometric Determination of Iron Content 分光光度法測(cè)定鐵含量 118
Expt. 17 Synthesis and Characterization of Three Kinds of Cobalt-ammine Coordination Compounds 三種鈷氨配合物的制備及表征 126
Expt. 18 Determination of Cement Composition 水泥組分測(cè)定 132
Expt. 19 Preparation and Determination of Three Kinds of Sodium Phosphate Hydrates 三種磷酸鈉鹽水合物的制備及測(cè)定 139
Expt. 20 Preparation of Heteropolyacid Salts and Determination of Conversion Kinetics 雜多酸鹽的制備及其轉(zhuǎn)化動(dòng)力學(xué)測(cè)定 144
APPENDIX 151
Appx. 1 Illustration of Common Glassware and Apparatus 常用玻璃器皿和儀器插圖 151
Appx. 2 Vocabulary of Common Professional Words and Phrases 常用專(zhuān)業(yè)詞匯中英文對(duì)照表 152
Appx. 3 Density, Content and Concentration of Common Concentrated Acids and Bases 常用濃酸、濃堿的密度、含量和濃度 157
Appx. 4 Common Indicators 常用指示劑 157
Appx. 5 Color of Common Ions and Inorganic Compounds 常見(jiàn)離子和無(wú)機(jī)化合物的顏色 159
Appx. 6 Bilingual Videos Embedded in the Manual 本書(shū)插入雙語(yǔ)視頻清單 160
Appx. 7 Atomic Weight of Elements 元素的原子量 162